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Food and Nutrition

Determination of Sodium Chloride in Foods and Other Samples by Quantab ™ Chloride Titrators

Laboratory Procedure MFLP-45
April 1997

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Health Protection Branch

Ottawa

Ashton Hughes and Tom Gleeson
Evaluation Division
Bureau of Microbial Hazards, Food Directorate
HPB, Address Locator 2204A1
Ottawa, Ontario KIA OL2

1. Application

This method can be used to determine chloride content of most foods. The kit will provide results as % sodium chloride or ppm Cl - on a wet weight bases. In order to determine % brine it will be necessary to determine the moisture content of the sample. If a regulation specifies an Official Method then that method should be followed such as MFO 38 for % salt in smoked fish products.

2. Principle

Quantab™ Chloride Titrators are convenient test devices used to measure the chloride content in aqueous solutions or dilute aqueous extracts of solids. These devices contain all the reagents necessary to carry out standard chloride titration. The titrators are pre-calibrated and provide quantitative results which are easy to read and interpret.

Quantab is a registered trademark of Environmental Test Systems, Inc., Ames Co. a Division of Miles Laboratories Inc., Elkhart, IN.

3. Definition of Terms

See Appendix A of Volume 3.

4. Collection of Samples

See Appendix B of Volume 3.

5. Materials and Special Equipment

1) The reagents for the Quantab ™ are provided in the kit, which is available from:

Fisher Scientific, 112 Colonnade Rd. Nepean, Ontario K2E 7L6 613-225-8874 or 1-800-267-3540; catalogue no AM 1176 or from: VWR 178 Hanson St. Toronto, Ontario, M4C 1A7, 416-699-5555 or 800-932-5000; catalogue no 66130-502

2) The method requires test tubes (16x100mm) [50 mL beakers may be substituted], filter paper (Whatman #1) and glass funnels